Citation: | HUANG Yan, LIN Lingchao, JIANG Tingting, et al. Simultaneous Determination of Vitamins A, D and E in Children's Formula Milk Powder by Combining Online Solid Phase Extraction and Two-Dimensional Liquid Chromatography[J]. Science and Technology of Food Industry, 2023, 44(9): 317−323. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2022060239 |
[1] |
贺媛媛, 贺陈龙, 李雅然, 等. 反复呼吸道感染患儿维生素A、D、E水平及免疫功能指标的相关性[J]. 贵州医科大学学报,2020,45(11):1347−1350. [HE Y Y, HE C L, LI Y R, et al. Correlation between the levels of vitamins A, D, E, and immune function indexes in children with recurrent respiratory infections[J]. Journal of Guizhou Medical University,2020,45(11):1347−1350.
|
[2] |
李兵, 赵海燕, 屠瑞莹, 等. 食品中维生素D与25-羟基维生素D检测技术及含量分布研究进展[J]. 分析测试学报,2019,38(4):495−502. [LI B, ZHAO H Y, TU R Y, et al. Recent advances on determination techniques for vitamin D and 25-hydroxyvitamin D and their content distributions in foods[J]. Journal of Instrumental Analysis,2019,38(4):495−502. doi: 10.3969/j.issn.1004-4957.2019.04.020
|
[3] |
纪建兵, 刘金祥, 王正军, 等. 血清维生素A和维生素E水平与小儿急性下呼吸道感染的相关性[J]. 解放军预防医学杂志,2019,37(2):136−138. [JI J B, LIU J X, WANG Z J, et al. Association between serum vitamin A and vitamin E levels and acute lower respiratory tract infection in children[J]. Journal of Preventive Medicine of Chinese People’s Liberation Army,2019,37(2):136−138. doi: 10.13704/j.cnki.jyyx.2019.02.051
|
[4] |
王慧, 毕颖薇. 特发性矮身材儿童血清维生素A及维生素D的水平研究[J]. 中华临床医师杂志,2021,15(6):445−449. [WANG H, BI Y W. Study of serum vitamin A and vitamin D level in idiopathic short stature children[J]. Chinese Journal of Clinicians,2021,15(6):445−449.
|
[5] |
FANALI C, D'ORAZIO G, FANALI S, et al. Advanced analytical techniques for fat-soluble vitamin analysis[J]. TrAC Trends in Analytical Chemistry,2017,87:82−97. doi: 10.1016/j.trac.2016.12.001
|
[6] |
WOOLLARD D C, BENSCH A, INDYK H, et al. Determination of vitamin A and vitamin E esters in infant formulae and fortified milk powders by HPLC: Use of internal standardization[J]. Food Chemistry,2016,197(A):457−465.
|
[7] |
魏帅, 吕宁, 梁成珠, 等. 婴幼儿配方乳粉中维生素A、E检测方法的比较研究[J]. 食品安全质量检测学报,2020,11(24):9083−9092. [WEI S, LÜ N, LIANG C Z, et al. Comparative study of analytical methods on vitamin A and vitamin E in infant formula[J]. Journal of Food Safety and Quality,2020,11(24):9083−9092. doi: 10.19812/j.cnki.jfsq11-5956/ts.2020.24.002
|
[8] |
GILL B D, INDYK H E. Analysis of vitamin D2 and vitamin D3 in infant and adult nutritional formulas by liquid chromatography-tandem mass spectrometry: A multilaboratory testing study[J]. Journal of AOAC International,2018,101(1):256−263. doi: 10.5740/jaoacint.17-0149
|
[9] |
中华人民共和国国家卫生和计划生育委员会, 国家食品药品监督管理总局. GB 5009.82-2016 食品安全国家标准食品中维生素A, D, E的测定[S]. 北京: 中国标准出版社, 2016
National Health and Family Planning Commission of the People's Republic of China, China Food and Drug Administration. GB 5009.82-2016 National food safety standard-Detemination of vitamin A, D, E in food[S]. Beijing: Standards Press of China, 2016.
|
[10] |
孙学文, 刘莹莹, 谢军, 等. 超高效液相色谱-串联质谱法同时测定特殊医学用途配方食品中5种脂溶性维生素[J]. 中国食品药品监管,2020(6):64−70. [SUN X W, LIU Y Y, XIE J, et al. Simultaneous determination of five fat-soluble vitamins in formula foods for special medical use by ultra performance liquid chromatography-tandem mass spectrometry[J]. China Food & Drug Administration Magazine,2020(6):64−70.
|
[11] |
施鹏飞, 王晓薇, 王巧云, 等. 超高效液相色谱法测定乳及乳制品中维生素D的含量[J]. 食品安全质量检测学报,2020,11(7):2122−2129. [SHI P F, WANG X W, WANG Q Y, et al. Determination of vitamin D in milk and dairy products by ultraperformance liquid chromatography[J]. Journal of Food Safety and Quality,2020,11(7):2122−2129. doi: 10.19812/j.cnki.jfsq11-5956/ts.2020.07.017
|
[12] |
吴新文, 马凯, 张世芹, 等. 高效液相色谱法同时测定婴幼儿配方乳粉中的维生素A、D3、E和β-胡萝卜素[J]. 食品安全导刊,2019(15):182−185. [WU X W, MA K, ZHANG S Q, et al. Simultaneous determination of vitamin A, D3, E and β-carotene in infant formula milk powder by high performance liquid chromatography[J]. China Food Safety Magazine,2019(15):182−185.
|
[13] |
黄旭, 袁波, 刘家阳. 固相萃取-高效液相色谱法测定婴幼儿乳粉中维生素D3的含量[J]. 山东化工,2017,46(8):82−84. [HUANG X, YUAN B, LIU J Y. Determination of vitamin D3 in infant milk powder by SPE-HPLC[J]. Shandong Chemical Industry,2017,46(8):82−84. doi: 10.3969/j.issn.1008-021X.2017.08.029
|
[14] |
程传民, 李云, 谷明, 等. 超高效液相色谱-串联质谱法测定饲料中维生素D3[J]. 中国饲料,2022(1):83−87. [CHENG C M, LI Y, GU M, et al. Determination of vitamin D3 in feed by ultra performance liquid chromatography-tandem mass spectrometry[J]. China Feed,2022(1):83−87.
|
[15] |
张艳海, 其布勒哈斯, 金燕, 等. 在线二维液相色谱法同时测定婴幼儿和成人配方营养品中的维生素A、D3和E[J]. 色谱,2015,33(3):291−297. [ZHANG Y H, QIBULE H, JIN Y, et al. Simultaneous determination of vitamins A, D3 and E in infant formula and adult nutritions by online two-dimensional liquid chromatography[J]. Chinese Journal of Chromatography,2015,33(3):291−297. doi: 10.3724/SP.J.1123.2014.11009
|
[16] |
赵玉富, 咸伟玥. 二维液相色谱法同时测定饲料中维生素A、维生素D3、维生素E[J]. 饲料博览,2019(4):51−54. [ZHAO Y F, XIAN W Y. Two-dimensional liquid chromatography method for the content determination of vitamin A, vitamin D3, vitamin E in feed[J]. Feed Review,2019(4):51−54. doi: 10.3969/j.issn.1001-0084.2019.04.013
|
[17] |
HUANG B F, PAN X D, ZHANG J S, et al. Determination of vitamins D2 and D3 in edible fungus by reversed-phase two-dimensional liquid chromatography[J]. Journal of Food Quality,2020,2020:1−6.
|
[18] |
林玉宙, 吴宏, 郭荣烁, 等. 二维液相色谱/双检测器法同时测定婴幼儿配方奶粉中维生素A、D3和E的含量[J]. 食品工业科技,2016,37(20):68−71, 77. [LIN Y Z, WU H, GUO R S, et al. Simultaneous determination of vitamin A, D3 and E in infant formula milk powder and rice flour by two dimensional liquid chromatography/double detector[J]. Science and Technology of Food Industry,2016,37(20):68−71, 77.
|
[19] |
赵玉富, 刘晓玲, 咸伟玥, 等. 二维液相色谱同时测定婴幼儿配方乳粉中多种脂溶性维生素[J]. 中国乳品工业,2019,47(6):37−40. [ZHAO Y F, LIU X L, XIAN W Y, et al. Simultaneous determination of various fat-soluble vitamin in infant formula milk powder by two dimensional liquid chromatography[J]. China Dairy Industry,2019,47(6):37−40. doi: 10.3969/j.issn.1001-2230.2019.06.009
|
[20] |
张丽媛, 戚绿叶, 周明昊, 等. 柱切换法液相色谱测定保健食品中的维生素A、D、E[J]. 食品科学,2021,13(5):46−48. [ZHANG L Y, QI L Y, ZHOU M H, et al. Determination of vitamin A, D and E in health food by column switching liquid chromatography[J]. Food Science,2021,13(5):46−48. doi: 10.7506/spkx1002-6630-20200924-292
|
[21] |
陈建彪. 在线净化二维液相色谱快速检测食品中维生素A、D、E[J]. 食品安全质量检测学报,2019,10(6):1726−1733. [CHEN J B. Rapid detection of vitamin A, D and E in food by on-line purification two-dimensional high performance liquid chromatography[J]. Journal of Food Safety and Quality,2019,10(6):1726−1733. doi: 10.3969/j.issn.2095-0381.2019.06.054
|
[22] |
FRANK J, CHIN X W D, SCHRADER C, et al. Do tocotrienols have potential as neuroprotective dietary factors?[J]. Ageing Research Reviews,2012,11:163−180. doi: 10.1016/j.arr.2011.06.006
|
[23] |
PAN J L, ZHANG C J, ZHANG Z M, et al. Review of online coupling of sample preparation techniques with liquid chromatography[J]. Analytica Chimica Acta,2014,815:1−15. doi: 10.1016/j.aca.2014.01.017
|
[24] |
DAVANKOV V, TSYURUPA M. Chapter 13-hypercrosslinked polystyrene as column packing material in HPLC[J]. Comprehensive Analytical Chemistry,2011,56:503−521. doi: 10.1016/S0166-526X(11)56013-1
|
[25] |
DZHABIEVA S A, KURBATOVA S V. Sorbent effect on retention of benzotriazoles in RP HPLC[J]. Russian Journal of Physical Chemistry A,2015,89(10):1907−1913. doi: 10.1134/S0036024415100088
|
[26] |
SYCHOW C S, ILYIN M M, DAVANKOV V A, et al. Elucidation of retention mechanisms on hypercrosslinked polystyrene used as column packing material for high-performance liquid chromatography[J]. Journal of Chromatography A,2004,1030(1−2):17−24. doi: 10.1016/j.chroma.2003.10.098
|
[27] |
DAVANKOV V A, TSYURUPA M P. Structure and properties of porous hypercrosslinked polystyrene sorbents styrosorb[J]. Pure and Applied Chemistry,1989,61(11):1881−1888. doi: 10.1351/pac198961111881
|
[28] |
SAIFUTDINOV B R, DAVANKOV V A, PETUKHOVA G A, et al. Thermodynamics of liquid-phase adsorption on hypercrosslinked polystyrene networks with ultimate degrees of crosslinking[J]. Doklady Physical Chemistry,2015,462(2):135−139. doi: 10.1134/S0012501615060056
|
[29] |
WU D, NEDEV G K, LUCY C A. Retention mechanism of hypercrosslinked polystyrene silic hybrid phase in normal phase chromatography[J]. Journal of Chromatography A,2014,1370:50−55. doi: 10.1016/j.chroma.2014.10.018
|
[30] |
WONG Y F, MAKAHLEH A, SAAD B, et al. UPLC method for the determination of vitamin E homologues and derivatives in vegetable oils, margarines and supplement capsules using pentafluorophenyl column[J]. Talanta,2014,130:299−306. doi: 10.1016/j.talanta.2014.07.021
|
[31] |
中华人民共和国国家质量监督检验检疫总局, 中国国家标准化管理委员会. GB/T 27404-2008 实验室质量控制规范 食品理化检测[S]. 北京: 中国标准出版社, 2008
General Administration of Quality Supervision, Inspection and Quarantine of China, Standardization Administration of China. GB/T 27404-2008 Criterion on quality control of laboratories-Chemical testing of food[S]. Beijing: Standards Press of China, 2008.
|