Rapid Detection of Cadmium and Arsenic in Dried <i>Auricularia auricula</i> by High Definition X-ray Fluorescence Spectrometry

WANG Yifan; YU Mingxin; PEI Longying; ZHAO Liyan

doi:10.13386/j.issn1002-0306.2022060260

Issue 9

May. 2023

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JOURNAL OF MECHANICAL ENGINEERING > 2023 > 44(9): 333-339.

WANG Yifan, YU Mingxin, PEI Longying, et al. Rapid Detection of Cadmium and Arsenic in Dried Auricularia auricula by High Definition X-ray Fluorescence Spectrometry[J]. Science and Technology of Food Industry, 2023, 44(9): 333−339. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2022060260

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WANG Yifan, YU Mingxin, PEI Longying, et al. Rapid Detection of Cadmium and Arsenic in Dried Auricularia auricula by High Definition X-ray Fluorescence Spectrometry[J]. Science and Technology of Food Industry, 2023, 44(9): 333−339. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2022060260

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Rapid Detection of Cadmium and Arsenic in Dried Auricularia auricula by High Definition X-ray Fluorescence Spectrometry

doi: 10.13386/j.issn1002-0306.2022060260

1.
College of Food Science and Technology, Nanjing Agricultural University, Nanjing 210095, China
2.
College of Food Science and Engineering, Xinjiang Institute of Technology, Akesu 843100, China

Received Date: 28 Jun 2022
Issue Publish Date: 01 May 2023

Abstract

Abstract

The contents of cadmium and arsenic in dried Auricularia auricula were rapidly detected by high definition X-ray fluorescence (HDXRF) spectrometry. In the process of the experiment, the dried Auricularia auricula samples were pre-treated, and the three experimental conditions of particle size, sample weight, and instrument measurement time were optimized. Figures of merit such as precision, reproducibility, and stability were evaluated. The results showed that, the optimal detection conditions of HDXRF were: particle size of 100 meshes, sample weight of 0.80 g, and measurement time of 600 s. This method allowed direct detection of cadmium and arsenic in 15 min, and a detection limit of 0.035 mg/kg of cadmium and 0.012 mg/kg of arsenic, respectively. The relative standard deviations (RSD) of precision, reproducibility and stability of HDXRF were all below 10%. Finally, the results of HDXRF were compared with inductively coupled plasma mass spectrometry (ICP-MS). The results were accurate and the relative errors were less than 20%. It indicates that the method of HDXRF can meet the rapid detection requirements of cadmium and arsenic in dried Auricularia auricula.
- high definition X-ray fluorescence (HDXRF) spectrometry,
- Auricularia auricula,
- cadmium,
- arsenic,
- rapid determination

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Rapid Detection of Cadmium and Arsenic in Dried Auricularia auricula by High Definition X-ray Fluorescence Spectrometry

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Rapid Detection of Cadmium and Arsenic in Dried Auricularia auricula by High Definition X-ray Fluorescence Spectrometry

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