干热处理对藜麦全粉结构及混粉面团流变学特性的影响

周亚丽; 游新勇; 李晓龙; 张坤朋; 李安华; 高靖雯; 刘萍; 朱梓瑜

doi:10.13386/j.issn1002-0306.2022060035

干热处理对藜麦全粉结构及混粉面团流变学特性的影响

doi: 10.13386/j.issn1002-0306.2022060035

安阳工学院生物与食品工程学院，河南安阳 455000

基金项目: 安阳工学院博士科研启动基金项目（BSJ2020019）；河南省重点研发与推广专项（藜麦全粉挤压膨化加工关键技术及其功能食品研发：212102110335）；基于学生深度参与为导向的田间试验与统计课程建设探索与实践（2020JGLX144）。

详细信息

作者简介:
周亚丽（1990−），女，博士，讲师，研究方向：农产品加工和天然产物的提取，E-mail：zyl@ayit.edu.cn

通讯作者:
游新勇（1982−），男，博士，讲师，研究方向：农产品加工、检测和天然产物的提取，E-mail：xinyong8206@163.com

中图分类号: TS211.4
计量
- 文章访问数: 16
- HTML全文浏览量: 21
- PDF下载量: 0
- 被引次数: 0
出版历程
- 收稿日期: 2022-06-05
- 刊出日期: 2023-05-01

Effect of Dry Heat Treatment on the Structure of Quinoa Flour and Rheological Properties of Dough

College of Biological and Food Engineering, Anyang Institute of Technology, Anyang 455000, China

摘要

摘要: 本研究以藜麦全粉为原料，分别进行常温（对照）、110、130、150 ℃干热处理1 h；将不同处理的藜麦粉15%与小麦粉85%（w/w）混合制作面包，分析干热处理温度对藜麦粉结构、混粉面团粉质特性、拉伸特性及面包质构特性、体外消化活性的影响。结果表明：干热处理使藜麦粉颗粒表面的聚集物脱落并出现缺陷，并且随着处理温度的升高，聚集物脱落的程度增加。干热处理未改变藜麦粉的A型晶型结构。与添加常温藜麦粉的面团相比，添加110、130、150 ℃干热处理藜麦全粉混粉面团的吸水率和弱化度分别升高1.79%和43.75%、3.25%和104.17%、4.83%和125.00%；延伸度、最大拉伸阻力和拉伸阻力均呈下降趋势，拉伸比呈现先升高后降低的趋势。干热处理温度为110 ℃时，面包硬度降低1.82%、弹性增加4.51%，而其他处理使面包硬度增加、弹性降低。干热处理使藜麦面包RDS含量显著降低，SDS和RS含量显著增加（P<0.05）。该研究结果可为藜麦粉功能性食品的研发提供理论依据。
- 藜麦粉 /
- 干热处理 /
- 面包 /
- 结构 /
- 品质
Abstract: Quinoa flour was subjected to dry heat treatment at room temperature (for control), 110, 130 and 150 ℃ for 1 h, respectively, and different treatments quinoa flour 15% and wheat flour 85% (w/w) were mixed to make bread, the effects of dry heat treatment temperature on the structure of quinoa flour, powder properties and tensile properties of the mixed flour dough as well as textural properties and in vitro digestive activity of the bread were analyzed. The results showed that the dry heat treatment caused the shedding of aggregates on the quinoa flour particles surface and caused defects, meanwhile the shedding degree of aggregates increased with the increase of treatment temperature. While, the crystal type of quinoa flour was not change and remained A-type after dry heat treatment. Compared with control, the water absorption and weakness of the dough that added quinoa flour treated with 110, 130 and 150 ℃ increased by 1.79% and 43.75%, 3.25% and 104.17%, 4.83% and 125.00%, respectively. Elongation, maximum tensile resistance and tensile resistance decreased gradually, and the tensile ratio increased first and then decreased. In addition, the bread hardness decreased by 1.82% and elasticity increased by 4.51% at 110 °C, while the other treatments increased the hardness and decreased the elasticity of quinoa-bread. Meanwhile, the dry heat treatment significantly decreased the RDS content and increased the SDS and RS content of quinoa-bread (P<0.05). This study can provide a theoretical basis for the development of functional foods from quinoa flour.
- quinoa flour /
- dry heat treatment /
- bread /
- structure /
- quality

HTML全文

图 1 不同干热处理温度的藜麦粉样品扫描电镜（SEM）图像

注：Bck：常温藜麦全粉；B110：110 ℃干热处理1 h的藜麦全粉；B130：130 ℃干热处理1 h的藜麦全粉；B150：150 ℃干热处理1 h的藜麦全粉；图2~图4，表1~表4同。

Figure 1. Scanning electron microscope （SEM） image of quinoa flour samples at different dry heat treatment temperature

下载: 全尺寸图片幻灯片

图 2 不同干热处理温度的藜麦粉样品X射线衍射图

Figure 2. X-ray diffraction patterns of quinoa flour samples at different dry heat treatment temperature

下载: 全尺寸图片幻灯片

图 3 不同干热处理温度的藜麦粉样品FT-IR光谱

Figure 3. FT-IR spectrum of quinoa flour samples at dry heat treatment temperature

下载: 全尺寸图片幻灯片

图 4 不同干热处理温度对面包硬度和弹性的影响

注：图中不同小写字母表示差异显著（P<0.05）。

Figure 4. Effects of different dry heat treatment temperature on hardness and elasticity of quinoa bread

下载: 全尺寸图片幻灯片

表 1 不同干热处理温度的藜麦粉样品相对结晶度

Table 1. Relative crystallinity of quinoa flour samples at different dry heat treatment temperature

	Bck	B110	B130	B150
相对结晶度（%）	38.56±0.38^d	41.35±0.38^c	42.68±0.38^ab	43.21±0.38^a
注：同行不同小写字母表示差异显著P<0.05，表2同。

下载: 导出CSV

表 2 不同干热处理温度对混粉面团粉质特性的影响

Table 2. Effect of different dry heat treatment temperature on farinograph properties of mixed dough

指标	不同干热处理样品
指标	Bck	B110	B130	B150
吸水率（%）	61.50±0.46^d	62.60±0.23^bc	63.50±0.17^ab	64.47±0.18^a
形成时间（min）	4.50±0.07^a	4.10±0.04^ab	3.20±0.05^c	2.40±0.08^d
稳定时间（min）	14.60±0.33^a	12.20±0.39^b	9.50±0.25^c	7.60±0.19^d
弱化度（FU）	48.00±1.33^d	69.00±1.36^c	98.00±2.58^b	108.00±3.88^a

下载: 导出CSV

表 3 不同干热处理温度对混粉面团拉伸特性的影响

Table 3. Effect of different dry heat treatment temperature on extensograph properties of mixed dough

指标	醒发时间	不同干热处理样品
指标	醒发时间	Bck	B110	B130	B150
延伸度（mm）	45 min	128.33±4.63^a	114.33±6.36^a	108.0±3.21^a	100.33±2.03^a
	90 min	120±3.06^ab	108±2.52^b	98.33±1.45^ab	63.67±1.20^c
	135 min	98.67±1.76^c	87.67±2.33^c	80.33±1.48^c	73.67±1.86^b
最大拉伸阻力（EU）	45 min	650.33±7.14^c	629.33±1.41^c	600.67±9.1^c	474.33±7.70^c
	90 min	834.0±1.82^b	814.67±1.62^b	797±9.66^b	634.33±6.12^ab
	135 min	898±5.13^a	854.67±5.96^a	806.33±3.54^a	644.670±9.21^a
拉伸阻力（EU）	45 min	486.33±3.48^c	465.33±4.33^c	441.67±6.64^c	397.67±2.17^c
	90 min	673.33±6.36^a	604.0±7.23^b	574.67±4.06^b	487.67±4.10^b
	135 min	567.00±3.79^b	625.33±4.91^a	696.0±9.07^a	502.67±6.64^a
拉伸比值	45 min	3.78±0.02^c	4.06±0.04^c	4.04±0.04^c	3.92±0.05^c
	90 min	5.71±0.02^ab	5.86±0.03^b	5.67±0.03^b	5.26±0.03^b
	135 min	5.79±0.01^a	8.66±0.03^a	7.18±0.02^a	6.71±0.05^a
注：同列不同小写字母表示差异显著（P<0.05），表4同。

下载: 导出CSV

表 4 不同干热处理温度对面包RDS、SDS和RS含量的影响

Table 4. Effects of different dry heat treatment temperature on the content of RDS, SDS and RS of quinoa bread

样品	RDS（%）	SDS（%）	RS（%）	SDS+RS（%）
Bck	50.12±0.19^a	25.90±0.18^d	28.67±0.17^d	54.57±0.42^d
B110	49.00±0.12^ab	27.71±0.14^a	30.50±0.12^c	58.21±0.32^bc
B130	48.04±0.12^bc	26.34±0.23^bc	32.09±0.31^b	58.43±0.40^b
B150	47.68±0.21^d	26.89±0.25^b	34.19±0.34^a	61.08±0.78^a

下载: 导出CSV

参考文献(33)

[1]	SALVATORE M, ALEXIS M V, MARJO K, et al. Effects of different drying temperatures on the content of phenolic compounds and carotenoids in quinoa seeds (Chenopodium quinoa Wild.) from finland[J]. Journal of Food Composition & Analysis,2018,72:75−82.
[2]	LI G, ZHU F. Quinoa starch: Structures, properties, and applications[J]. Carbohydrate Polymers,2017,181:851−861.
[3]	GAWLIK-DZIKI U, DZIKI D, SWIECA M, et al. Bread enriched with Chenopodium quinoa leaves powder-The procedures for assessing the fortification efficiency[J]. LWT-Food Science and Technology,2015,62(2):1226−1234. doi: 10.1016/j.lwt.2015.02.007
[4]	周亚丽, 崔利华, 陈建光, 等. 黑, 白藜麦皂苷的提取及其抗氧化活性的比较[J]. 食品工业科技,2021,42(11):328−334. [ZHOU Y L, CUI L H, CHEN J G, et al. Extraction of saponins from black and white quinoa and comparison of their antioxidant activities[J]. Science and Technology of Food Industry,2021,42(11):328−334.
[5]	BILATU A, RUTH B, LEGESSE S. Quinoa (Chenopodium quinoa, Wild.): As a potential ingredient of injera in Ethiopia[J]. Journal of Cereal Science,2018,82:170−174. doi: 10.1016/j.jcs.2018.06.009
[6]	SEZGIN A C, SANLIER N. A new generation plant for the conventional cuisine: Quinoa (Chenopodium quinoa Willd.)[J]. Trends in Food Science & Technology,2019,86:51−58.
[7]	ELIANA P, CHRISTIAN E Z, BARROS L, et al. Chemical and nutritional characterization of Chenopodium quinoa Willd (quinoa) grains: A good alternative to nutritious food[J]. Food Chemistry,2019,280:110−114. doi: 10.1016/j.foodchem.2018.12.068
[8]	XU X J, LUO Z G, YANG Q Y, et al. Effect of quinoa flour on baking performance, antioxidant properties and digestibility of wheat bread[J]. Food Chemistry,2019,294(OCT.1):87−95.
[9]	SHEWRY P R, HEY S J. The contribution of wheat to human diet and health[J]. Food Energy Security,2015,4(3):178−202. doi: 10.1002/fes3.64
[10]	ALLER E, ABETE I, ASTRUP A, et al. Starches, sugars and obesity[J]. Nutrients,2011,3(3):341−369. doi: 10.3390/nu3030341
[11]	SENAY S, MARIBEL O M, ALI M, et al. Chemical composition, digestibility and emulsification properties of octenyl succinic esters of various starches[J]. Food Research International,2015,75:41−49. doi: 10.1016/j.foodres.2015.05.034
[12]	CHUNG H J, QIANG L, HOOVER R. Impact of annealing and heat-moisture treatment on rapidly digestible, slowly digestible and resistant starch levels in native and gelatinized corn, pea and lentil starches[J]. Carbohydrate Polymers,2009,75(3):436−447. doi: 10.1016/j.carbpol.2008.08.006
[13]	FLORES-SILVA P C, ROLDAN-CRUZ C A, CHAVEZ-ESQUIVEL G, et al. In vitro digestibility of ultrasound-treated corn starch[J]. Starch‐Starke,2017,69(9-10):1700040. doi: 10.1002/star.201700040
[14]	HUNG P V, HUONG N, PHI N, et al. Physicochemical characteristics and in vitro digestibility of potato and cassava starches under organic acid and heat-moisture treatments[J]. International Journal of Biological Macromolecules,2017,95:299−305.
[15]	SUN Q, GONG M, LI Y et al. Effect of dry heat treatment on the physicochemical properties and structure of proso millet flour and starch[J]. Carbohydr Polym,2014,110:128−134. doi: 10.1016/j.carbpol.2014.03.090
[16]	OH I K, YOUNG B I, GYU L H. Effect of dry heat treatment on physical property and in vitro starch digestibility of high amylose rice starch[J]. International Journal of Biological Macromolecules,2018,108:568−575. doi: 10.1016/j.ijbiomac.2017.11.180
[17]	PRABA K S, DIVYA P, USHA A. Effect of dry heat treatment on the development of resistant starch in rice (Oryza sativa) and barnyard millet (Echinochloa furmantacea)[J]. Journal of Food Processing & Preservation,2019,43(7):e13965.1−e13965.7.
[18]	LIU K, HAO Y, CHEN Y, et al. Effects of dry heat treatment on the structure and physicochemical properties of waxy potato starch[J]. International Journal of Biological Macromolecules,2019,132:1044−1050. doi: 10.1016/j.ijbiomac.2019.03.146
[19]	ZHOU Y L, CUI L H, YOU X Y, et al. Effects of repeated and continuous dry heat treatments on the physicochemical and structural properties of quinoa starch[J]. Food Hydrocolloids,2020,113:106532.
[20]	SUDHA M L, SOUMYA C, PRABHASANKAR P. Use of dry-moist heat effects to improve the functionality, immunogenicity of whole wheat flour and its application in bread making[J]. Journal of Cereal Science,2016,69:313−320. doi: 10.1016/j.jcs.2016.04.010
[21]	PEREZ I C, MU T H, ZHANG M, et al. Effect of heat treatment to sweet potato flour on dough properties and characteristics of sweet potato-wheat bread[J]. Food Science and Technology International,2017,23:708−715. doi: 10.1177/1082013217719006
[22]	XU J, ZHANG W, ADHIKARI K, et al. Determination of volatile compounds in heat-treated straight-grade flours from normal and waxy wheats[J]. Journal of Cereal Science,2017,75:77−83. doi: 10.1016/j.jcs.2017.03.018
[23]	WANG M, WU Y, LIU Y, et al. Effect of ultrasonic and microwave dual-treatment on the physicochemical properties of chestnut starch[J]. Polymers,2020,12(8):1718. doi: 10.3390/polym12081718
[24]	梁霞, 孟婷婷, 周柏玲, 等. 藜麦-小麦粉的流变学特性及其面条研制[J]. 现代食品科技,2020,36(7):184−192. [LIANG X, MENG T T, ZHOU B L, et al. Rheological properties of quinoa-wheat flour and development of its noodles[J]. Modern Food Science and Technology,2020,36(7):184−192.
[25]	ENGLYST H N, KINGMAN S M, CUMMINGS J H. Classification and measurement of nutritionally important starch fractions[J]. European Journal of Clinical Nutrition,1992,46:S33−S50.
[26]	GONZÁLEZ M, VERNON-CARTER E J, ALVAREZ-RAMIREZ J, et al. Effects of dry heat treatment temperature on the structure of wheat flour and starch in vitro digestibility of bread[J]. International Journal of Biological Macromolecules,2021,166:1439−1447. doi: 10.1016/j.ijbiomac.2020.11.023
[27]	吴昊. 反复/连续干热处理对不同晶型淀粉结构及理化特性的影响[D]. 杨凌: 西北农林科技大学, 2019 WU H. Effect of repeated/continuous dry heat treatments on structural and physicochemical properties of different crystal types of starches[D]. Yangling: Northwest A&F University, 2019
[28]	YING D Y, HLAING M M, LERISSON J, et al. Physical properties and FTIR analysis of rice-oat flour and maize-oat flour based extruded food products containing olive pomace[J]. Food Research International,2017,100(1):665−673.
[29]	王伟玲. 干热加工对小麦粉的性质影响及其机制探讨[D]. 合肥: 合肥工业大学, 2020 WANG W L. Properties of dry-heated wheat flour and its mechanism[D]. Hefei: Hefei University of Technology, 2020
[30]	CONTRERAS-JIMENEZ B, TORRES-VARGAS O L, RODRIGUEZ-GARCIA M E. Physicochemical characterization of quinoa (Chenopodium quinoa) flour and isolated starch[J]. Food Chemistry,2019,298(15):124982.1−124982.7.
[31]	杜文娟, 吕静, 申瑞玲, 等. 小米粉对面团流变学特性的影响[J]. 粮食与油脂,2016,29(4):33−36. [DU W J, LÜ J, SHEN R L, et al. Effects of millet flour on the rheological properties of dough[J]. Cereals and Oils,2016,29(4):33−36. doi: 10.3969/j.issn.1008-9578.2016.04.010
[32]	金鑫. 南方馒头品质评价、原料选择及工艺研究[D]. 长沙: 湖南农业大学, 2020 JIN X. Study on quality evaluation, wheat flour selection and processing of southern-style steamed bread[D]. Changsha: Hunan Agricultural University, 2020
[33]	LIU K, ZHANG B, CHEN L, et al. Hierarchical structure and physicochemical properties of highland barley starch following heat moisture treatment[J]. Food Chemistry,2019,271:102−108. doi: 10.1016/j.foodchem.2018.07.193